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Ball-on-three-balls test

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Sketch of the B3B test setup (specimen Ø 20 mm, loading ball Ø 13 mm) with preload applied, after guide ring is lowered.[1]

The ball-on-three-balls test (B3B test) is a mechanical testing method for determining the biaxial strength of brittle materials. It involves placing a disc- or plate-shaped specimen on three supporting balls arranged in an equilateral triangle and applying a compressive force to the centre of the opposite face using a fourth ball. This setup produces a biaxial stress field that more closely simulates real-world multiaxial loading conditions compared to uniaxial tests, and it allows for testing of as-sintered or unpolished surfaces.

It is designed to simulate multiaxial stress conditions, offering a more application-relevant measure of strength than traditional uniaxial tests. Compared to conventional three- or four-point flexural tests, the B3B test offers several advantages, including reduced sensitivity to geometrical inaccuracies, minimal influence from edge defects, and low friction effects. These characteristics make it particularly suitable for testing small-sized specimens.[2] Variations of the test were made, including the B3B- test and the three-balls-on-three-balls (3-on-3) test. They are particularly used in ceramic engineering, electroceramics and dental materials.

History

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Initial work on the ball-on-three-balls (B3B) test began in the 1980s and was subsequently expanded by Austrian materials scientist Andreas Börger et al.[3][4] Earlier methods, such as the ring-on-ring (RoR) and ball-on-ring (BoR) tests, were already in use but presented limitations related to stress uniformity, specimen preparation, and the sensitivity to geometric imperfections like surface curvature or waviness.[2] The B3B test configuration was introduced as a modification of the ball-on-ring setup, which supports the specimen with a continuous ring.[5]

Test method

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The B3B test is a biaxial flexural strength testing method developed for brittle materials,[6] such as ceramics and cementitious materials,[7] in the form of discs or plates.[8] The test is intended to replicate multiaxial stress states, providing strength measurements that more closely reflect real-world loading conditions compared to conventional uniaxial testing methods.[9] In the B3B test, the specimen—typically a circular disc or a rectangular plate[8]—is supported on its underside by three equally spaced spherical balls that form an equilateral triangle.[10] The specimen is then loaded on the opposite side by a fourth ball, which is positioned centrally to the three supporting balls,[10][8] applies a compressive force to the centre of the opposite face.[11] The four balls are typically of the same size.[10][8] This symmetric configuration results in a biaxial stress field in the specimen, with the maximum tensile stress occurring at the centre of the supported face.[10][11]

The test is generally conducted by gradually increasing the load until the specimen fractures.[12] Fixture designs often include radial grooves to position the support balls and centring pins or screws to align the specimen.[13] A small preload (typically 10% of the expected fracture load) may be applied initially to stabilise the setup before loading begins.[14]: 1271  The B3B test is often compared to the Small Punch Test (SPT), as both use miniature disc specimens. While the SPT involves clamping the specimen and deforming it with a small punch, the B3B test offers a contact geometry that is more suitable for testing unmachined or as-sintered surfaces.[15]: 962 

The test setup often includes precision alignment aids such as centring rings and a punch mechanism that transmits load from a mechanical testing machine. Components in contact with the specimen are usually made from high-purity aluminium oxide (Al2O3), ensuring chemical and mechanical stability during testing.[16]: 595–6 

Procedure

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Testing is typically performed under displacement control at a constant rate until the specimen fails. The load is recorded continuously using a load cell. From the critical load at fracture, the maximum tensile stress can be calculated using analytical equations or finite element models.[16]: 595 

High-temperature testing is possible using specialized furnaces, with reported extensions up to 1,400–1,600 °C (2,550–2,910 °F).[16]: 595  An argon gas environment is often employed to prevent oxidation or decarburization during elevated-temperature tests.[16]: 586 

Stress analysis

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The B3B test induces a multiaxial stress state, which is more representative of real-world conditions such as thermal shock or contact loading. The maximum principal tensile stress at the specimen centre is used to define the material's biaxial strength. For linear elastic discs, this stress () is calculated using the equation:[17][18]

where is the applied force, is the thickness of the specimen, and is a dimensionless geometry factor determined by finite element method (FEM). This factor depends on specimen and support geometry as well as the material's Poisson's ratio (ν).[17][18] FEM has been extensively used to derive empirical formulae for stress evaluation across a wide range of materials and geometries.[19]

The B3B test lends itself to statistical strength analysis, often based on the Weibull distribution. This accounts for the size effect in brittle fracture, where larger specimens typically exhibit lower average strength due to the increased likelihood of critical flaws. Because the stress field in the B3B test is non-uniform, equivalent stress criteria—such as the principle of independent action (PIA) or the maximum principal stress criterion—are used to interpret the data.[15]: 964 

Variations

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B3B-KIc test

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The B3B test can be adapted for fracture toughness () testing by introducing a specimen that is supported by three equidistant balls and loaded on the opposite face by a fourth, centrally positioned ball. A semielliptical surface crack on the loaded face of the specimen. After applying a small preload, the load is increased until fracture, and the crack dimensions are analysed post-failure.[8]

Conventional fracture toughness tests require relatively large specimens, which may be unsuitable for materials processed in small quantities or in thin geometries. The B3B- method addresses this limitation by using circular or rectangular plate specimens and integrating a precrack to enable linear elastic fracture mechanics (LEFM)-based evaluation.[12] When combined with simulations (e.g., FEM or cohesive zone model), B3B results can be used to extract fracture toughness values and fit cohesive parameters by comparing simulated and experimental load–deflection curves.[16]: 595–6 

The fracture toughness is calculated using the Griffith–Irwin equation:[12]

Here, is the maximum tensile stress from the B3B configuration, is the crack depth, and is a dimensionless geometric factor derived via FEM. Because varies and depends on specimen and crack geometry as well as the Poisson's ratio ν. For semicircular or semielliptical surface cracks, varies along the crack front, and the maximum value is used for evaluating toughness. Calculated values for ​ at various parameter combinations are available in the literature for ν = 0.3.[12]

can be expressed by empirical formula:[12]

where the dimensionless factor accounts for the specimen's geometry through three dimensionless parameters: the thickness-to-radius ratio (), the loading radius-to-specimen radius ratio (), and the Poisson's ratio (ν). Although originally intended for circular discs, an effective specimen radius can also be calibrated for rectangular plates. The loading radius () is determined by the ball diameter () of the four balls, given as .[12]

Accurate positioning of the crack is essential, as lateral misalignment can lead to significant overestimation of . However, rotational misalignment has negligible effect on test results.[20]

Three-balls-on-three-balls test

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A modified three-balls-on-three-balls (3B3B) version uses three balls for both the loading and supporting forces. This variant of the test was patented in 2004 to expand the effective high-stress region on the specimen surface, addressing one of the limitations of the original B3B setup.[21]

For a specific case where the loading and supporting balls are aligned and the disk geometry has a radius ratio , the maximum principal stress ​ can be estimated using the following empirical relation derived from finite element analysis:[22]

Here, is the applied force, the specimen thickness, the specimen radius, and ν the Poisson's ratio. The expressions serve as a dimensionless geometric factor specific to the 3B3B arrangement and highlights the reduced stress concentration resulting from load distribution across three points.[22]

The three-on-three configuration may also vary in terms of alignment, with some designs positioning the loading and supporting balls directly in line and others offset by angular displacements such as 60 degrees.[21] FEM has been used to analyse stress states in this variation, which has shown significantly reduced maximum principal stresses for the same total load compared to the one-on-three B3B test.[23]

Applications

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The B3B test and its variations are widely used for evaluating the strength and toughness of brittle materials, including:

Its tolerance for surface roughness[26] and geometric imperfections[1] makes it well-suited for as-sintered samples,[15]: 966  providing a practical solution for industrial quality assurance and rapid screening.[1]

References

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  1. ^ a b c Harrer et al. 2008, p. 1271.
  2. ^ a b Börger, Supancic & Danzer 2002, p. 1425.
  3. ^ Staudacher et al. 2021, p. 3.
  4. ^ Börger, Supancic & Danzer 2002, pp. 1425–36.
  5. ^ Fett et al. 2007, pp. 2–4.
  6. ^ Danzer et al. 2007, p. 1481.
  7. ^ Fu & Weiss 2020, p. 128.
  8. ^ a b c d e Lube, Rasche & Nindhia 2016, p. 249.
  9. ^ Fett et al. 2007, p. 1.
  10. ^ a b c d Danzer et al. 2007, p. 1482.
  11. ^ a b Börger, Andreas; Danzer, Robert; Supancic, Peter (2004). "Biaxial Strength Test of Discs of Different Size Using the Ball on Three Balls Test". In Lara-Curzio, Edgar; Readey, Michael J. (eds.). 28th International Conference on Advanced Ceramics and Composites B. Ceramic Engineering and Science Proceedings. Vol. 25. Hoboken, NJ, USA: John Wiley & Sons, Inc. pp. 283–288. doi:10.1002/9780470291191.ch43. ISBN 978-0-470-29119-1.
  12. ^ a b c d e f Lube, Rasche & Nindhia 2016, p. 250.
  13. ^ Fett et al. 2007, p. 3.
  14. ^ Harrer, Walter; Danzer, Robert; Supancic, Peter; et al. (2008). The Ball on Three Balls Test: Strength Testing of Specimens of Different Sizes and Geometries. Proceedings of the 10th International Conference of the European Ceramic Society. pp. 1271–1275. ISBN 3-87264-022-4.
  15. ^ a b c Rasche, Stefan; Strobl, Stefan; Kuna, Meinhard; et al. (2014). "Determination of Strength and Fracture Toughness of Small Ceramic Discs Using the Small Punch Test and the Ball-on-three-balls Test". Procedia Materials Science. 20th European Conference on Fracture. 3: 961–966. doi:10.1016/j.mspro.2014.06.156. ISSN 2211-8128.
  16. ^ a b c d e Aneziris, Christos G.; Biermann, Horst (2024). Multifunctional Ceramic Filter Systems for Metal Melt Filtration. Springer Series in Materials Science. Vol. 337. Cham: Springer Nature. doi:10.1007/978-3-031-40930-1. ISBN 978-3-031-40930-1. ISSN 0933-033X – via the Internet Archive.
  17. ^ a b Börger, Supancic & Danzer 2002, p. 1429.
  18. ^ a b Harrer et al. 2008, p. 1272.
  19. ^ Börger, Supancic & Danzer 2002, pp. 1429–30.
  20. ^ Lube, Rasche & Nindhia 2016, p. 254.
  21. ^ a b Fett et al. 2007, p. 5.
  22. ^ a b Fett et al. 2007, pp. 14–5.
  23. ^ Fett et al. 2007, pp. 9.
  24. ^ a b Danzer et al. 2007, p. 1483.
  25. ^ Wendler, Michael; Belli, Renan; Petschelt, Anselm; et al. (2017). "Chairside CAD/CAM materials. Part 2: Flexural strength testing". Dental Materials. 33 (1): 99–109. doi:10.1016/j.dental.2016.10.008. ISSN 0109-5641.
  26. ^ Börger, Supancic & Danzer 2002, p. 1434.

Bibliography

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